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Rotary Evaporators, Heidolph

(1) General properties of the Laborate 4000 series

Safety

  • Control panel is below the handles for the heating bath, for protection from vapour and splashes
  • All heating baths have handles with anti-slip pads for protection against scalds
  • Heating baths with double wall for your protection against burns and insulation against heat loss
  • No open heating coil in the bath for protection against burns and for quick cleaning
  • Optional safety cover protects you from implosions and splashes and can be adjusted horizontally with the bath
  • Extension plate for an expanded horizontal adjustment (up to 210 mm) for highest stability
  • Upon request, glass sets for implosion protection also with completely transparent plastic coating (Surlyn® coated)

 

Operation comfort

  • Long-life and highly resistant vacuum seal made of PTFE with graphite filling
  • Guaranteed no blocking of the glass hollow shafts in the drive due to non-sticking plastic grippers
  • Set-up to push off stuck pistons
  • Fixing the max. immersion depth to any height with one movement
  • The angle of the evaporator piston can be changed from 10° to 85° with one movement
  • All models available with hand lift or motor lift upon request
  • Long life-span, 3 year warranty

 

Laborota 4000 eco

  • Low-cost model with hand lift & water bath
  • Big, easy-to-operate turning knobs to set the rotation speed and the heating bath temperature
  • Rotation speed from 20 to 270 1/min
  • Safety due to separate main switch for temperature and rotation speed
  • Water bath: temperature range from 20 – 100°C, control accuracy from ± 2,5°C
  • Available with 3 glass sets

 

 ArticleVersionGlassware
 standardcoated
 Order No.€/pcOrder No.€/pc
 Laborota eco 4000/HB/G1diagonal condenser10 41 9031010 41 90311
 Laborota eco 4000/HB/G3vertical condenser10 41 9033010 41 90331
 Laborota eco 4000/HB/G5condension trap10 41 9035010 41 90351



(2) Laborota efficient

Laborota 4000 efficient with hand lift / Laborota 4001 efficient with motor lift

  • Big, easy-to-operate turning knobs to set rotation speed and heating bath temperature
  • Rotation speed 20 – 270 1/min
  • Universal heating bath for water and oil: temperature range 20°C to 180°C, control accuracy ± 1°C
  • Safety due to separate main switch for temperature and rotation speed
  • Exact display of the set target temperature in the display
  • Automatic distillation control can be added with optional vacuum control Vac control automatic

 

 Laborota efficientVersionGlassware
 standardcoated
 Order No.€/pcOrder No.€/pc
 4000/HB/G1diagonal condenser57 41 9011010 41 90111
 4000/HB/G3vertical condenser57 41 9013010 41 90131
 4000/HB/G5condensation trap57 41 9015010 41 90151
 4000/HB/G6reflux distillation57 41 9016010 41 90161
 4001/HB/G1diagonal condenser57 41 9111010 41 91111
 4001/HB/G3vertical condenser57 41 9113010 41 91131
 4001/HB/G5condensation trap57 41 9115010 41 91151
 4001/HB/G6reflux distillation57 41 9116010 41 91161



(3) Laborota digital

Laborota 4010 digital with hand lift / Laborota 4011 digital with motor lift

 

As Laborota 4000 / 4001 but with:

  • Digital display of the rotation speed, vapour temperature and heating bath temperature
  • Accuracy of the vapour temperature display: ± 0,1°C
  • Vapour temperature probe already included

 

 Laborota digitalVersionGlassware
 standardcoated
 Order No.€/pcOrder No.€/pc
 4010/HB/G1diagonal condenser57 41 9411010 41 94111
 4010/HB/G3vertical condenser57 41 9413010 41 94131
 4010/HB/G5condensation trap57 41 9415010 41 94151
 4010/HB/G6reflux distillation57 41 9416010 41 94161
 4011/HB/G1diagonal condenser57 41 9511010 41 95111
 4011/HB/G3vertical condenser57 41 9513010 41 95131
 4011/HB/G5condensation trap57 41 9515010 41 95151
 4011/HB/G6reflux distillation57 41 9516010 41 95161



(4) Laborota control

Laborota 4002 control with hand lift / Laborota 4003 control with motor lift

 

As Laborota 4010 / 4011 but with:

  • Integrated vacuum control with 3 programmes for automatic distillation
  • Programme P(const) (control parameter: pressure) for vacuum control for material separation. With this programme, the vacuum can be kept at a constant level by means of the push of a button at any time during evacuation
  • Programme T(auto) (control parameter: vapour temperature) for vacuum control for distillation of solution mixtures. This programme automatically cancels distillation if a defined end pressure is not met.
  • The Programme P(auto) automatically looks for the required vacuum for a boiling point and keeps it at a constant level (combination of T(auto) and P(const))
  • Digital setting of the required bath temperature, of the vacuum, the timer function and the control parameters for automatic distillation
  • Digital display of the rotation speed, bath temperature, vacuum and vapour temperature
  • Safety temperature for heat bath, for overheat protection, separately selectable
  • With a push of a button, rotation, vacuum control and timer can be started
  • Up to 9 data records of frequently used distillation parameters can be saved
  • The required change of the vacuum can be programmed as ramp

 

 Laborota controlVersionGlassware
 standardcoated
 Order No.€/pcOrder No.€/pc
 4002/HB/G1diagonal condenser57 41 9211010 41 92111
 4002/HB/G3vertical condenser57 41 9213010 41 92131
 4002/HB/G5condensation trap57 41 9215010 41 92151
 4002/HB/G6reflux distillation57 41 9216010 41 92161
 4003/HB/G1diagonal condenser57 41 9311010 41 93111
 4003/HB/G3vertical condenser57 41 9313010 41 93131
 4003/HB/G5condensation trap57 41 9315010 41 93151
 4003/HB/G6reflux distillation57 41 9316010 41 93161



Rotacool chillers

Maximal performance in minimal space.

  • The only chiller designed specifically for rotary evaporators
  • Minimal bench space thanks to unique L-shape design
  • Chillers base 470 × 580 mm
  • Provides space of 470 × 405 mm for the evaporator 
  • Temperature range -10°C up to +40°C
  • Cooling capacity:
    at 15°C 400 W
    at 0°C 300 W
    at -10°C 270 W
  • Small quantity of circulating coolant required due to innovative control
  • High control accuracy (± 0.5 K)
  • CFC-free

 

 ArticleOrder No.
(5) Rotacool chiller56 41 00200



Rotacool chillers

  • Circulation cooler for all standard rotary evaporators
  • Little need for space: 225 × 450 mm
  • Cooling temperature (fixed): 7°C
  • Temperature consistency: 1°C
  • CFC-free

 

 ArticleOrder No.
(6) Rotacool mini chiller10 41 10021



Vacuum pumps

Vacuum pump Rotavac valve tec

  • Valve-controlled vacuum pump suitable for all Heidolph rotary evaporators
  • 2-tier membrane pump made of chemical-resistant material
  • Suction power at 50Hz 0.75 m³/h (at 60Hz 0.9 m³/h)
  • Maximum end pressure 12 mbar
  • Can be combined with a condensate cooler to condense residue solvents

 

Vacuum pump Rotavac valve control

  • Valve-controlled vacuum pump suitable for all Heidolph rotary evaporators
  • Sufficient suction power for 3 rotary evaporators at the same time
  • 2-tier membrane pump made of chemical-resistant material
  • High suction power from 1.7 m3/h, for quick evacuation
  • Maximum end pressure of 9 mbar
  • Can be combined with a condensate cooler to condense residue solvents

 

Vacuum pump Rotavac vario tec

  • Revolution-controlled vacuum pump suitable for combination with Laborota control 4002 / 4003
  • 2-tier membrane pump made of chemical-resistant material
  • Suction power of 1.0 m³/h, for quick evacuation
  • Maximum end pressure 12 mbar
  • Automatic adjustment of the suction volume to the distillation process
  • 30% shortened process times
  • Optimal solvent recovery of up to 100%
  • Low-noise, low-vibration
  • Can be combined with a condensate cooler to condense residue solvents

 

Vacuum pump Rotavac vario control

  • Revolutions-controlled vacuum pump suitable for combination with Laborota control 4002 / 4003
  • 3-tier membrane pump made of chemical-resistant material
  • High suction power of 1.5 m3/h, for quick evacuation
  • Maximum end pressure of 2 mbar
  • Automatic adjustment of the suction volume to distillation process
  • 30% shortended process times
  • Optimal solvent recovery of up to 100%, no delay in boiling
  • Low-noise, low-vibration
  • Can be combined with a condensate cooler to condense residue solvents

 

 ArticleOrder No.
(7) Rotavac valve control56 41 10130
(8) Rotavac vario control56 41 10140
 Condensate cooler for Rotavac valve control56 41 10081
 Condensate cooler for Rotavac vario control56 41 10082
(9) Vacuum pump Rotavac valve tec10 41 10016
(10) Vacuum pump Rotavac vario tec10 41 10017
 Condensate cooler for Rotavac valve & vario tec10 41 10008



Vacuum controller Vac control automatic

Vacuum controller for retrofitting to Laborota efficient and digital

  • For controlling your house vacuum or any other existing vacuum pumps
  • Timer for distillation period
  • Reduces pressure during distillation
  • Convenient mounting with lift column
  • Includes vacuum sensor and valve
  • Controller automatically finds required vacuum and holds vacuum constant
  • Connections for vacuum valve and switchbox, which are available as accessories

 

 ArticleOrder No.
(11) Vac control automatic56 41 10340



Accessories

Switchbox

Connect up to 3 rotary evaporators to one pump and control vacuum individually.

  • Vacuum pump switches off automatically when no vacuum required
  • Reduces energy consumption of pump
  • Increases pump performance life
  • Vacuum valve and check valve are required for every evaporator if you work with different pressures at the same time

 

Vac senso T

Required for Laborota control models with valve regulated pumps.

  • Includes power supply for vacuum valve, vacuum sensor and vent valve
  • Controls vacuum with and accuracy of ± 0.5%
  • Opens vacuum valve at the end of the application
  • Vacuum valve is connected to Vac senso T, connection for switchbox is integrated
  • All components in contact with vapor are made of chemical-resistant PTFE, PVDF and stainless steel 1.4305

Vacuum valve

Required for Laborota control models with valve regulated pumps.

  • External construction designed for easy cleaning
  • Can be combined with the Woulff Bottle to make one unit (optional)
  • For separating condensate after the condenser in order to protect the valves of the vacuum pump

 

Woulff Bottle

  • For separating condensate after the condenser in order to protect the valves of the vacuum pump
  • Easy connection along side the lift column
  • Direct connection to the vacuum valve
  • Third connection for the vacuum line to the vacuum controller
  • Capacity of 250 ml

 

 ArticleOrder No.
 Switch box56 41 00040
 Vac senso T56 41 00035
 Vacuum valve56 41 00024
 Woulfe bottle56 41 00070



Accessories for Laborota 4000 series

 

 ArticleOrder No.
 Vapor temperature sensor10 41 10003
 

for Laborota efficient

 
 Temperature sensor T(auto)10 41 10004
 for Laborota control 
 Guard hood10 41 10001
 Strong guard hood to protect you from implosions 
 Guard shield10 41 10002
 for your protection while changing flasks 
 Tube set10 41 13500
 consists of 5 meters vacuum hose and 6 meters water hose 
 Extension kit for heating bath10 41 10009
 Heating bath liquid 5 l51 41 93100
 with water mixable, max. temperature 240°C, 5 l 



Complete systems

  • Different package solutions adapted to the customers' requirements
  • Attractive price advantage against modular orders of individual components
  • Simplified order process via only one article number
  • Perfectly adjusted system components
  • Package include all accessories necessary for operation

Complete packages PREMIUM

Automatic distillation with revolution-controlled vacuum control

 

All PREMIUM packages include:

  • a rotary evaporator Laborota 4002 or 4003 with universal heating bath and glass set
  • revolutions-controlled vacuum pump with condensate cooler Rotavac vario tec or vario control
  • temperature cooler T(auto)
  • coil set

 

 ArticleVersionOrder No.
 Premium 1 TLR 4002, vertical condenser, Rotavac vario tec10 41 86130
 Premium 3 TLR 4002, reflux condenser, Rotavac vario tec10 41 86160
 Premium 4 TLR 4002, vertical condenser (coated), Rotavac vario tec10 41 86131
 Premium 6 TLR 4002, reflux condenser (coated), Rotavac vario tec10 41 86161
 Premium 4 TCMLR 4002, vertical condenser (coated), Rotavac vario tec, Rotacool mini10 41 86132
 Premium 1LR 4002, vertical condenser, Rotavac vario control10 41 96130
 Premium 3LR 4002, reflux condenser, Rotavac vario control10 41 96160
 Premium 4LR 4002, vertical condenser (coated), Rotavac vario control10 41 96131
 Premium 6LR 4002, reflux condenser (coated), Rotavac vario control10 41 96161
 Premium 7LR 4003, vertical condenser, Rotavac vario control10 41 97130
 Premium 9LR 4003, reflux condenser, Rotavac vario control10 41 97160
(12) Premium 10LR 4003, vertical condenser (coated), Rotavac vario control10 41 97131
 Premium 10 coolLR 4003, vertical condenser (coated), Rotavac vario control, Rotacool10 41 97132
 Premium 12LR 4003, reflux condenser (coated), Rotavac vario control10 41 97161



Further packages from the categories BASIC (low-cost packages with water bath), STANDARD (standard applications) and SUPERIOR (automatic distillation with valve-controlled vacuum control) available upon request!

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